Monochloramine → 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride
Reaktionsgleichung
[CH3:1][CH:2]1[O:7][CH:6]([CH3:8])[CH2:5][N:4]([CH2:9][CH:10](O)C)[CH2:3]1.[Cl:13]N>>[ClH:13].[Cl:13][CH2:10][CH2:9][N:4]1[CH2:3][CH:2]([CH3:1])[O:7][CH:6]([CH3:8])[CH2:5]1Komponenten
3
Versuchsvorschrift
An amount, 389.3 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.25 moles) was condensed with the free chloroamine obtained from 481.5 grams N-chloroethyl-2,6-dimethylmorpholine hydrochloride (2.25 moles) as described above to give 415.9 grams (58.8%) of the catalyst, bp 127°-129° C. at 0.3 mm of Hg. The structure was confirmed as that of the title compound by elemental analysis, calc. 64.9 C, 10.9 H, 8.9 N; found 64.4 C, 10.6 H, 8.9 N.
Quellen und Nachweise
- ORD-Eintrag
- ord-2bf37e33554e4fd9b07d5dfa61613237
- Quelldatensatz
- uspto-grants-1987_11
- Patentnummer
- US04705840
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