HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Decanol → 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Decanol | HCID 8174 | — |
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 2-Dimethylaminopyridine | HCID 21885 | — |
| Edukt | 2,6-Naphthalenedicarbonyl dichloride | HCID 3485596 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride | HCID 54316020 | 56,3% |
Reaktionsschritte
After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05207947 |
| Quelldatensatz | uspto-grants-1993_05 |
| ORD ID | ord-75e52ba2a4e54b1da4dfeb4197a82b67 |
| Quellennotiz | uspto-grants-1993_05 |