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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 247796Erstellt: 25. Oktober 2026

1-Decanol → 2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chloride

https://huagongshe.com/reaction/247796

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-DecanolHCID 8174—
EduktTriethylamineHCID 8471—
Edukt2-DimethylaminopyridineHCID 21885—
Edukt2,6-Naphthalenedicarbonyl dichlorideHCID 3485596—
LösungsmittelDichloromethaneHCID 6344—
Produkt2-n-Decyloxycarbonylnaphthalene-6-carboxylic acid chlorideHCID 5431602056,3%

Reaktionsschritte

After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05207947
Quelldatensatzuspto-grants-1993_05
ORD IDord-75e52ba2a4e54b1da4dfeb4197a82b67
Quellennotizuspto-grants-1993_05