HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chloroethane → N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chloroethane | HCID 6337 | — |
| Edukt | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide | HCID 9890945 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride | HCID 19764599 | — |
Reaktionsschritte
5.5 g of the compound obtained in stage A is taken up in 10 cm3 of acetonitrile. 7.5 cm3 of a 3.3N solution of hydrochloric ether are added to this solution. 3.1 g of a solid which corresponds to the title compound are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05208243 |
| Quelldatensatz | uspto-grants-1993_05 |
| ORD ID | ord-5e7f19ff56af4ccabb05d3f49423a133 |
| Quellennotiz | uspto-grants-1993_05 |