1-Iodododecane → alpha-Methyl-6-(dodecyloxy)-2-naphthaleneacetic acid
Reaktionsgleichung
I[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[OH:14][C:15]1[CH:16]=[C:17]2[C:22](=[CH:23][CH:24]=1)[CH:21]=[C:20]([CH:25]([CH3:29])[C:26]([OH:28])=[O:27])[CH:19]=[CH:18]2>>[CH3:29][CH:25]([C:20]1[CH:19]=[CH:18][C:17]2[C:22](=[CH:23][CH:24]=[C:15]([O:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH3:2])[CH:16]=2)[CH:21]=1)[C:26]([OH:28])=[O:27]Komponenten
3
Versuchsvorschrift
The title compound is prepared according to the method of Example 7 using 1-iodododecane and racemic 6-hydroxy-α-methyl-2-naphthaleneacetic acid. White crystals are obtained having a melting point of 96°-97° C.
Aufarbeitung
- customWhite crystals are obtained
Quellen und Nachweise
- ORD-Eintrag
- ord-beb4777bc4914dea9d11846edd54790a
- Quelldatensatz
- uspto-grants-1993_05