HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 5-(4-chlorophenyl)furan-2-carbonyl Chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 5-(4-Chlorophenyl)-2-furoic acid | HCID 726693 | — |
| Produkt | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
Reaktionsschritte
A mixture Of 56 g. (0.25 mole) Of 5-(p-Chlorophenyl)-2furoic acid and 100 ml. of SOCl2 is refluxed for 31/2 hours so that HCl gas evolves and there is dissolution. The SOCl2 is removed on a rotary evaporator. Benzene is added to the solid residue and is then removed on the rotary evaporator to give 5-(p-chlorophenyl)-2-furoyl chloride
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05214042 |
| Quelldatensatz | uspto-grants-1993_05 |
| ORD ID | ord-6d5c33762e0b4b7bbe1d8dfa22e751fe |
| Quellennotiz | uspto-grants-1993_05 |