Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 249267Erstellt: 25. Oktober 2026

Acetone → 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol

https://huagongshe.com/reaction/249267

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetoneHCID 180—
Edukt4-Propyl-1,2-benzenediolHCID 97638—
Eduktp-Toluenesulfonic acid monohydrateHCID 521998—
LösungsmittelBenzeneHCID 241—
Produkt5-n-Propyl-2,2-dimethyl-1,3-benzodioxolHCID 15165616—

Reaktionsschritte

The same procedures as described in Example 10 were carried out by using a mixture of 7.61 g (50 mM) of 4-n-propylcatechol, 15 ml of acetone, 30 mg of p-toluenesulfonic acid monohydrate and 15 ml of benzene. 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol was obtained in the yield of 9.13 g (47 mM) as colorless transparent liquid having a boiling point of 82°-87° C./3 mmHg.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05214034
Quelldatensatzuspto-grants-1993_05
ORD IDord-7dca0d1e7733477f968a6c1bcbc5a80b
Quellennotizuspto-grants-1993_05