Hydrochloric Acid → HCID 22569398, Verbindung

HRID 24942Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 24942
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH2:15].Cl>C(O)C>[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH:15][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 9590p-FluoronitrobenzeneHCID 66053N,N-Dimethylethylenediamine

Produkt 1

HCID 22569398HCID 22569398, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

2.2 ml of (20 mmol) of 4-fluoronitrobenzene and 2.6 ml (24 mmol) of N,N-dimethylethylene-diamine are heated in 10 ml of ethanol at 120° C. in a microwave oven for 1.5 hours. Then 50 ml of 1 N hydrochloric acid are added. The reaction solution is washed with ethyl acetate. Then the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction is obtained and extracted with ethyl acetate.

Aufarbeitung

  1. washThe reaction solution is washed with ethyl acetate
  2. customThen the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction
  3. customis obtained
  4. extractionextracted with ethyl acetate

Quellen und Nachweise

ORD-Eintrag
ord-33970417aed54766919fad76ccaaf316
Quelldatensatz
uspto-grants-2005_02
Patentnummer
US06855710B2

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