Ethyl Lactate → 3,7-Dimethyl-1-octyl lactate

HRID 249640

Reaktionsgleichung

Reaktionsgleichung von HRID 249640
[CH3:1][CH:2]([CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])[CH3:10])[CH2:3][CH2:4][OH:5].[C:12](OCC)(=[O:16])[CH:13]([CH3:15])[OH:14]>>[C:12]([O:5][CH2:4][CH2:3][CH:2]([CH3:1])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])[CH3:10])(=[O:16])[CH:13]([CH3:15])[OH:14]

Komponenten

3

Edukt 2

HCID 7344Ethyl LactateHCID 77923,7-Dimethyl-1-octanol

Produkt 1

HCID 115359583,7-Dimethyl-1-octyl lactateAusbeute 62,2 %

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

A mixture of Novozym 435 (2.81 g), molecular sieves (23.17 g), 3,7-dimethyl-1-octanol (4.64 g), and ethyl lactate (14.78 g) in a 250 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.2 g of 3,7-dimethyl-1-octyl lactate (62% yield) was obtained as an amber-colored liquid. The purity of the product was >96% as assessed by HPLC-RI.

Quellen und Nachweise

ORD-Eintrag
ord-5ef4352b11c3443e87db73d3185b8e02
Quelldatensatz
uspto-grants-2011_01
Patentnummer
US07863025B2

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