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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 249783Erstellt: 25. Oktober 2026

Trifluoroacetohydrazide → HCID 178446280, Verbindung

https://huagongshe.com/reaction/249783

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrifluoroacetohydrazideHCID 229753—
Eduktmethyl 4-(pentylamino)-1H-imidazole-5-carbimidothioateHCID 135984704—
LösungsmittelEthanolHCID 702—
ProduktHCID 178446280HCID 178446280—

Reaktionsschritte

The mixture of methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate (0.53 g, 2.4 mmol) and trifluoroacetic acid hydrazide (0.45 g, 3.5 mmol) in ethanol (10 mL) was refluxed overnight. The reaction mixture was concentrated to yield the product as slightly green viscous oil. LCMS calculated for C11H16F3N6(M+H): 289.1. found: 289.1.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07863285B2
Quelldatensatzuspto-grants-2011_01
ORD IDord-ae3d46556d5a4d618146d09e700d6d6f
Quellennotizuspto-grants-2011_01