HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trifluoroacetohydrazide → HCID 178446280, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trifluoroacetohydrazide | HCID 229753 | — |
| Edukt | methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate | HCID 135984704 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178446280 | HCID 178446280 | — |
Reaktionsschritte
The mixture of methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate (0.53 g, 2.4 mmol) and trifluoroacetic acid hydrazide (0.45 g, 3.5 mmol) in ethanol (10 mL) was refluxed overnight. The reaction mixture was concentrated to yield the product as slightly green viscous oil. LCMS calculated for C11H16F3N6(M+H): 289.1. found: 289.1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07863285B2 |
| Quelldatensatz | uspto-grants-2011_01 |
| ORD ID | ord-ae3d46556d5a4d618146d09e700d6d6f |
| Quellennotiz | uspto-grants-2011_01 |