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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 252474Erstellt: 26. Oktober 2026

Propiolic Acid → 1-Dodecyl-1H-1,2,3-triazole-4-carboxylic acid

https://huagongshe.com/reaction/252474

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPropiolic AcidHCID 10110—
Edukt1-AzidododecaneHCID 10998318—
Produkt1-Dodecyl-1H-1,2,3-triazole-4-carboxylic acidHCID 63467685—

Reaktionsbedingungen

Temperatur120 °C

Reaktionsschritte

A mixture of propiolic acid (46 μL, 0.7419 mmol) and 1-azido-dodecane (156.8 mg, 0.7419 mmol) was heated to 120° C. in a capped vial for 14 h, to yield the title triazole as white, crystalline solid (189.3 mg, 91% yield). The product was used without further purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07868135B2
Quelldatensatzuspto-grants-2011_01
ORD IDord-eb3be02f342142e3bc24729ff2e33713
Quellennotizuspto-grants-2011_01