HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodine → ethyl (NZ)-N-[4-butyl-2-(1,1,1-trifluoro-2-methylpropan-2-yl)-1,2-thiazol-5-ylidene]carbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodine | HCID 807 | — |
| Edukt | Hexanal | HCID 6184 | — |
| Edukt | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Edukt | 1,1,1-Trifluoro-2-methylpropan-2-amine | HCID 11275188 | — |
| Produkt | ethyl (NZ)-N-[4-butyl-2-(1,1,1-trifluoro-2-methylpropan-2-yl)-1,2-thiazol-5-ylidene]carbamate | HCID 87184182 | — |
Reaktionsschritte
Commercially available hexanal (Aldrich), 1,1,1-trifluoro-2-methylpropan-2-amine (Chemcollect), O-ethyl carbonisothiocyanatidate (Aldrich) and iodine were processed using the method described in Example 110A to afford the title compound. MS (ESI+) m/z 339 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07872033B2 |
| Quelldatensatz | uspto-grants-2011_01 |
| ORD ID | ord-4288e9071d894b849c100c13d51a098f |
| Quellennotiz | uspto-grants-2011_01 |