HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → HCID 42629230, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 3,5-Dichlorophenylboronic acid | HCID 2734331 | — |
| Edukt | 1-Bromo-8-fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline | HCID 57732452 | — |
| Katalysator | HCID 178418397 | HCID 178418397 | — |
| Produkt | HCID 42629230 | HCID 42629230 | 78% |
Reaktionsschritte
Following the general Suzuki coupling procedure, reaction of bromide 5A (75 mg, 0.25 mmol), 3,5-dichlorophenylboronic acid (58 mg, 0.30 mmol), K2CO3 (105 mg, 0.75 mmol) and Pd(PPh3)4 (5.8 mg, 0.005 mmol) provided the coupling product as a white powder (70 mg, 78% yield). EIMS 360.0 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07875618B2 |
| Quelldatensatz | uspto-grants-2011_01 |
| ORD ID | ord-87425095fd3243bf8895ea79040d8ade |
| Quellennotiz | uspto-grants-2011_01 |