HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thiophosgene → [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thiophosgene | HCID 10040 | — |
| Edukt | 5-(1H-indol-2-yl)-2-methoxy-phenylamine | HCID 9900204 | — |
| Produkt | [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate | HCID 22568433 | — |
Reaktionsschritte
The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06858739B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-0fec09881fb740ff8ab79f4f7634b1cd |
| Quellennotiz | uspto-grants-2005_02 |