1-(2-Nitropropoxy)-2,2,5,5-tetramethylcyclopentane → HCID 13878920, Verbindung
Reaktionsgleichung
[N+:1]([CH:4]([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14])([O-])=O>CO.[Ni]>[NH2:1][CH:4]([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14]Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
1-(2-Nitropropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-aminopropoxy)-2,2,5,5-tetramethylcyclopentane.
Aufarbeitung
- filtrationThe reaction mixture is filtered through Celite
- customevaporated
Quellen und Nachweise
- ORD-Eintrag
- ord-c237420f04314ad38502463442e85d65
- Quelldatensatz
- uspto-grants-1987_10
- Patentnummer
- US04698231
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