HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chloroanthraquinone → Anthrimide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chloroanthraquinone | HCID 6709 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | Disperse Violet 1 | HCID 31420 | — |
| Katalysator | Cuprous chloride | HCID 62652 | — |
| Lösungsmittel | Nitrobenzene | HCID 7416 | — |
| Produkt | Anthrimide | HCID 6700 | — |
Reaktionsschritte
Following the procedure as descrilbed in Example 1, but suspending the 1-chloroanthraquinone, 1,4-diaminoanthraquinone, sodium carbonate and CuCl in 300 ml of nitrobenzene, the anthrimide is obtained in a yield corresponding to that of Example 1. When following a conventional procedure, i.e. mixing the components and heating them slowly, if such a concentrated reaction mixture is employed, the reaction can no longer be carried out in an agitator vessel.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04701281 |
| Quelldatensatz | uspto-grants-1987_10 |
| ORD ID | ord-a3d0b1a6bb41422fb40fef4e3f3f4b93 |
| Quellennotiz | uspto-grants-1987_10 |