HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Nitroanthraquinone → 9,10-Anthracenedione, 1-(cyclohexylamino)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Nitroanthraquinone | HCID 6704 | — |
| Edukt | Cyclohexylamine | HCID 7965 | — |
| Lösungsmittel | 1,2-Dichlorobenzene | HCID 7239 | — |
| Produkt | 9,10-Anthracenedione, 1-(cyclohexylamino)- | HCID 70669 | — |
Reaktionsschritte
1-Nitroanthraquinone is refluxed with an excess of cyclohexylamine in o-dichlorobenzene to yield 1-cyclohexylamino anthraquinone which is further brominated in aqueous pyridine to yield the corresponding 1-cyclohexylamino-4-bromoanthraquinone. This compound is further condensed with p-amino acetanilide to yield 1-cyclohexylamino-4-(p-acetaminoanilino)anthraquinone as a bright green pleochroic dye having an optical order parameter 0.7.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04702561 |
| Quelldatensatz | uspto-grants-1987_10 |
| ORD ID | ord-fa9d28333a2f4b8088371292a34028d3 |
| Quellennotiz | uspto-grants-1987_10 |