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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 256277Erstellt: 24. Oktober 2026

1-Chloro-4-hydroxyanthraquinone → 1-Hydroxyanthraquinone

https://huagongshe.com/de/reaction/256277

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-Chloro-4-hydroxyanthraquinoneHCID 66510—
Edukt4-CyclohexylbenzenamineHCID 80764—
EduktSodium AcetateHCID 517045—
KatalysatorCupric acetateHCID 8895—
LösungsmittelNitrobenzeneHCID 7416—
Produkt1-HydroxyanthraquinoneHCID 8512—

Reaktionsschritte

The pleochroic dye 1-cyclohexylphenylamino, 4-hydroxyanthraquinone was prepared by combining equimolar quantities of 1-chloro-4-hydroxy anthraquinone and 4-cyclohexylaniline and heating in the presence of a catalytic amount of copper acetate (0.1 g/0.1 mole) and sodium acetate (10 g/0.1 mole) in nitrobenzene. The reaction was run and the dye separated and tested as in Example 70. The dye had an absorption maxima at 594 nm and an optical order parameter of 0.75.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04702561
Quelldatensatzuspto-grants-1987_10
ORD IDord-4036e1c133394fe891b76e93ce871235
Quellennotizuspto-grants-1987_10