Chlorotrimethylsilane → 1,1'-((1,1,3,3-Tetrakis((trimethylsilyl)oxy)-1,3-disiloxanediyl)di-3,1-propanediyl) bis(2-methyl-2-propenoate)

HRID 256456

Reaktionsgleichung

[C:1]([O:6][CH2:7][CH2:8][CH2:9][Si:10]([O:15]C)([O:13]C)[O:11]C)(=[O:5])[C:2]([CH3:4])=[CH2:3].Cl[Si:18]([CH3:21])([CH3:20])[CH3:19]>>[C:1]([O:6][CH2:7][CH2:8][CH2:9][Si:10]([O:13][Si:18]([CH3:21])([CH3:20])[CH3:19])([O:11][Si:18]([CH3:21])([CH3:20])[CH3:19])[O:15][Si:10]([CH2:9][CH2:8][CH2:7][O:6][C:1](=[O:5])[C:2]([CH3:4])=[CH2:3])([O:11][Si:18]([CH3:21])([CH3:20])[CH3:19])[O:13][Si:18]([CH3:21])([CH3:20])[CH3:19])(=[O:5])[C:2]([CH3:4])=[CH2:3]

Komponenten

Edukt 2

HCID 6397Chlorotrimethylsilane

HCID 173183-(Trimethoxysilyl)propyl methacrylate

Produkt 1

HCID 27567311,1'-((1,1,3,3-Tetrakis((trimethylsilyl)oxy)-1,3-disiloxanediyl)di-3,1-propanediyl) bis(2-methyl-2-propenoate)

Versuchsvorschrift

1.3-Bis(γ-methacryloxypropyl)-1,1,3,3-tetra(trimethylsiloxy)disiloxane (TETRA) was prepared following the same procedure as in Example (b) with 0.1 mole of γ-methacryloxypropyltrimethoxysilane (MEMO) and 0.2 mole of chlorotrimethylsilane.

Quellen und Nachweise

ORD-Eintrag: ord-92f7ee7f39bc43c09cfbd3b07ed05afc
Quelldatensatz: uspto-grants-1987_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04703097

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