Hydrochloric Acid → HCID 53977328, Verbindung

HRID 256464Notizen

Reaktionsgleichung

[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]=[O:6].Cl.[C:8](=[O:11])([O-])[O-].[Na+].[Na+].[CH3:14]O>>[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]([O:11][CH3:8])[O:6][CH3:14]

Komponenten

Edukt 4

HCID 313Hydrochloric Acid

HCID 887Methanol

HCID 10340Sodium Carbonate

HCID 537074664-Chlorobut-2-enal

Produkt 1

HCID 53977328HCID 53977328, Verbindung

Versuchsvorschrift

4-Chloro-1,1-dimethyoxy-2-butene (Reagent K) was prepared by reacting 7.46 g. of 4-chloro-2-butenal with 200 ml. of anhydrous methanol and a catalytic amount of hydrochloric acid. The reaction mixture was stirred at room temperature for 16 hours, neutralized with sodium carbonate, filtered, and concentrated.

Aufarbeitung

filtrationfiltered
concentrationconcentrated

Quellen und Nachweise

ORD-Eintrag: ord-063d2bb45b8947eda8c257c5d731e7ae
Quelldatensatz: uspto-grants-1987_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04703116

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