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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 256788Erstellt: 26. Oktober 2026

Cyclohexanone → Prop-2-enenitrile--ethenylbenzene (1/1)

https://huagongshe.com/reaction/256788

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCyclohexanoneHCID 7967—
EduktIsoquinolineHCID 8405—
KatalysatorCopper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)HCID 24350—
LösungsmittelN-methyl-2-pyrrolidoneHCID 13387—
ProduktProp-2-enenitrile--ethenylbenzene (1/1)HCID 6269610%

Reaktionsschritte

A solution of 2.0 g. CuI, 1.4 g. isoquinoline (1:1 ratio), 50.0 g. N-methylpyrrolidone solvent, 46.6 g. cyclohexanone and 0.20 g. Lustran SAN 31-1,000 (10% on CuI) was prepared. The resulting coating solution was coated on 7 mil raw PET with number 10 Meyer rod and dried three minutes at 240° F. The coating had very good uniformity and clarity and was gold and blue iridescent and lustrous. The resistivity measured 13-20×107 Ω/sq. The solution after time showed some precipitation, which crystals were redissolved upon reheating.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05259992
Quelldatensatzuspto-grants-1993_11
ORD IDord-3110b0bfc3814e4280160de68cfb5d7b
Quellennotizuspto-grants-1993_11