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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 256837Erstellt: 25. Oktober 2026

2-Bromopyridine → rac-3,4-Dihydro-2,5,7,8-tetramethyl-2-[(2-pyridinyl)ethynyl]-2H-1-benzopyran-6-ol

https://huagongshe.com/reaction/256837

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-BromopyridineHCID 7973—
Eduktrac-3,4-dihydro-2-ethynyl-2,5,7,8-tetramethyl-2H-1-benzopyran-6olHCID 14478563—
Produktrac-3,4-Dihydro-2,5,7,8-tetramethyl-2-[(2-pyridinyl)ethynyl]-2H-1-benzopyran-6-olHCID 15171815—

Reaktionsschritte

This compound was prepared by reacting rac-3,4-dihydro-2-ethynyl-2,5,7,8-tetramethyl-2H-1-benzopyran-6-ol with 2-bromopyridine as described in Example 14. The compound was isolated by chromatography as in Example 14 and was crystallized from ethyl acetate to give colorless crystals with m.p. 179°-181° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05260294
Quelldatensatzuspto-grants-1993_11
ORD IDord-0e4093ea66ba44b08c047f32de6b472e
Quellennotizuspto-grants-1993_11