HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075239 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 3-(3-Cyclopropylmethoxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075467 | — |
Reaktionsschritte
A mixture of methyl iodide (0.25 ml, 4 mmol) and 3-(4-cyclopropylmethoxy-1,2,5-thiadiazol-3-yl) pyridine (400 mg, 1.7 mmol) in acetone (5 ml) was stirred at room temperature for 36 h. The title compound precipitated from the solution and was collected by filtration to yield 0.41 g (65%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05260311 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-4835428e4bb145a3a6add907166a394a |
| Quellennotiz | uspto-grants-1993_11 |