4-Ethylpyridine → 1-(2-Fluorophenyl)-3-(4-pyridyl)-butane
Reaktionsgleichung
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[F:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[CH2:12][CH2:13]Br>>[F:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[CH2:12][CH2:13][CH:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2]Komponenten
3
Versuchsvorschrift
1.0 g (9.35 mmol) of 4-ethylpyridine and 1.90 g (9.35 mmol) of 2-fluorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified, to obtain 0.74 g of desired compound (yield: 39.2%).
Aufarbeitung
- customThe reaction product was purified
Quellen und Nachweise
- ORD-Eintrag
- ord-fd8adcaacb1a48c6a99eba5034a642b8
- Quelldatensatz
- uspto-grants-1993_11
- Patentnummer
- US05262420
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