HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Ethylpyridine → 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Ethylpyridine | HCID 10822 | — |
| Edukt | 2-(2-Bromoethyl)-1,3-dichlorobenzene | HCID 13480195 | — |
| Produkt | 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane | HCID 19783313 | 55,3% |
Reaktionsschritte
1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,6-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.45 g of the desired compound (yield: 55.3%). The resulting compound was identified as 1-(2,6-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 11) by the following analytical results.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05262420 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-ee4c7f6b2d9949818626607b3a34d2d8 |
| Quellennotiz | uspto-grants-1993_11 |