HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl acetone → (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl acetone | HCID 17355 | — |
| Edukt | 3-Ethyl-4-methylpyridine | HCID 68254 | — |
| Produkt | (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene | HCID 14883803 | 69,5% |
Reaktionsschritte
The procedure of Example 41 was repeated with the exception that 3.5 g of benzyl acetone in place of cinnamic aldehyde and 2.26 g of 3-ethyl-4-methylpyridine were used in Example 41, to obtain 3.26 g (yield: 59.8%) of (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl -1-butene (hereinafter referred to as compound 55) and o.95 g (yield: 17.4%) of (Z)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene (hereinafter referred to as compound 56). The analytical results are shown below.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05262420 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-8b990d7f82d54f9b834fc6ef6159ea3e |
| Quellennotiz | uspto-grants-1993_11 |