HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyldioxirane → 1-Hydroxy-2,6-diphenyl-3,5-dimethylpiperidin-4-yl Laurate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyldioxirane | HCID 115197 | — |
| Edukt | 2,6-Diphenyl-3,5-dimethylpiperidin-4-yl Laurate | HCID 53685275 | — |
| Produkt | 1-Hydroxy-2,6-diphenyl-3,5-dimethylpiperidin-4-yl Laurate | HCID 53668762 | 99,5% |
Reaktionsschritte
The general procedure of Example 2 is repeated using 29.9 g (64.5 mmol) of 2,6-diphenyl-3,5-dimethylpiperidin-4-yl laurate and 1.24 L (64.5 mmol) of dimethyldioxirane (0.050M in acetone). 30.8 g (98% yield) of the title compound is isolated: mp 108°-112° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05262538 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-dd0c233a7279440fa75c447a9c74ed5d |
| Quellennotiz | uspto-grants-1993_11 |