HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
m-Chloroperbenzoic acid → 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy](1,2-epoxy) styrol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | m-Chloroperbenzoic acid | HCID 70297 | — |
| Edukt | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol | HCID 18359165 | — |
| Lösungsmittel | Cyclohexane ethylacetate | HCID 21867204 | — |
| Produkt | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy](1,2-epoxy) styrol | HCID 18359067 | 99,6% |
Reaktionsschritte
Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05728828 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-3ce42197cace4f5dad3160cf94f08e0c |
| Quellennotiz | uspto-grants-1998_03 |