HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Phenylethanethiol → 6-Biphenyl-2-yl-2,2-dimethyl-4-phenethylsulfanylmethyl-1,2-dihydroquinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Phenylethanethiol | HCID 78126 | — |
| Edukt | Biphenyl-2-boronic acid | HCID 4589187 | — |
| Edukt | Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester | HCID 20760320 | — |
| Produkt | 6-Biphenyl-2-yl-2,2-dimethyl-4-phenethylsulfanylmethyl-1,2-dihydroquinoline | HCID 10367062 | — |
Reaktionsschritte
Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester was coupled with 2-biphenylboronic acid. Bromination and coupling reaction with 2-phenylethanethiol gave 57 mg of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06858627B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-c19277094bb64775bc862ab3379cb694 |
| Quellennotiz | uspto-grants-2005_02 |