2-Phenylethanethiol → 2,2-Dimethyl-6-(2-methylsulfanylphenyl)-4-phenethylsulfanylmethyl-1,2-dihydroquinoline

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-Phenylethanethiol	HCID 78126	—
Edukt	2-(Methylthio)benzeneboronic acid	HCID 2773543	—
Edukt	Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester	HCID 20760320	—
Produkt	2,2-Dimethyl-6-(2-methylsulfanylphenyl)-4-phenethylsulfanylmethyl-1,2-dihydroquinoline	HCID 10455467	—

Reaktionsschritte

Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester was coupled with 2-(methylthio)phenylboronic acid. Bromination and coupling reaction with 2-phenylethanethiol gave 59 mg of the title compound.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06858627B2
Quelldatensatz	uspto-grants-2005_02
ORD ID	ord-7038e07fd43c47049bcde43c3da206c3
Quellennotiz	uspto-grants-2005_02