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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 258463Erstellt: 24. Oktober 2026

Isobutyronitrile → 2,9-Dicyano-2,9-dimethyldecane

https://huagongshe.com/de/reaction/258463

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIsobutyronitrileHCID 6559—
EduktDiisopropylamineHCID 7912—
Edukt1,6-DibromohexaneHCID 12368—
Edukt2-Cyano-2-methyleicosaneHCID 19781207—
EduktButyllithiumHCID 178418339—
LösungsmittelTetrahydrofuranHCID 8028—
Produkt2,9-Dicyano-2,9-dimethyldecaneHCID 19781205—

Reaktionsschritte

By the procedure used to prepare the compound of Example 2, the title compound is prepared from 24 mL of a 2.5M n-butyllithium solution in hexanes, 6.07 g of diisopropylamine, 5.5 mL of isobutyronitrile, 7.32 g of 1,6-dibromohexane, and 120 mL of tetrahydrofuran. The IR and 1H NMR spectra of the white solid (7.7 g) obtained were consistent with structure of the desired product.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05266726
Quelldatensatzuspto-grants-1993_11
ORD IDord-0ebf857b948a47fc993f27b4d2982bd9
Quellennotizuspto-grants-1993_11