HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl orthoformate → Ethyl 1-(4-Chlorophenyl)-1,6-dihydro-2,4-dimethyl-6-oxopyrimidine-5-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl orthoformate | HCID 31214 | — |
| Edukt | Triethyl orthoacetate | HCID 66221 | — |
| Edukt | Ethyl 3-amino-2-(4-chlorophenylcarbamoyl)crotonate | HCID 70610046 | — |
| Produkt | Ethyl 1-(4-Chlorophenyl)-1,6-dihydro-2,4-dimethyl-6-oxopyrimidine-5-carboxylate | HCID 21325489 | 42% |
Reaktionsschritte
This compound is prepared in 42% yield from ethyl 3-amino-2-(4-chlorophenylcarbamoyl)crotonate in a manner analogous to Example 1 substituting triethyl orthoacetate for triethyl orthoformate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04147528 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-507868586bd341fa949a7da51d5fcec3 |
| Quellennotiz | uspto-grants-1979_04 |