HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-Dimethylbenzylamine → HCID 21425139, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-Dimethylbenzylamine | HCID 7681 | — |
| Edukt | Trichloropentylsilane | HCID 7885 | — |
| Edukt | alpha-Bromoethyltriethoxysilane | HCID 21425138 | — |
| Lösungsmittel | Methyl Ethyl Ketone | HCID 6569 | — |
| Produkt | HCID 21425139 | HCID 21425139 | — |
Reaktionsschritte
In a manner like that used for the preparation of alpha-bromoethyltriethoxysilane, alpha-bromoamyltriethoxysilane is prepared in two steps from amyltrichlorosilane (commercially available). One-quarter mole of alpha-bromoamyltriethoxysilane (78.5g) is refluxed for 12 hours with 0.25 moles (33.75g) of benzyldimethylamine in 125 ml. of 2-butanone. The product, alpha-(benzyldimethylammonio)ethyltriethoxysilane bromide is isolated by removing the solvent under vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04035411 |
| Quelldatensatz | uspto-grants-1977_07 |
| ORD ID | ord-c4e838e1b7d3491287275096ae3d8e91 |
| Quellennotiz | uspto-grants-1977_07 |