Acrylamide → Acrylamide 2-Methacryloyloxyethyl Trimethyl Ammonium
Reaktionsgleichung
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:11][CH2:12][CH2:13][N+:14]([CH3:17])([CH3:16])[CH3:15])(=[O:10])[C:7]([CH3:9])=[CH2:8]>>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:11][CH2:12][CH2:13][N+:14]([CH3:17])([CH3:15])[CH3:16])(=[O:10])[C:7]([CH3:9])=[CH2:8]Komponenten
3
Versuchsvorschrift
Acrylamide (AM) (49.6 g.), 2-methacryloyloxyethyl trimethyl ammonium methosulfate (METAMS) (26.0 g. of a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.) were combined and reacted according to the procedure of Example 31. The pH of the emulsion was adjusted to 6.0; the maximum temperature reached was 71° C.; the product was a stable emulsion.
Aufarbeitung
- distillationof a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.)
- customreacted
- customreached was 71° C.