Phosgene → 27676-61-5

HRID 259479Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 259479
[CH:1]([N:4]=[C:5]([CH3:7])[CH3:6])([CH3:3])[CH3:2].C(N(CC)CC)C.[C:15](Cl)([Cl:17])=[O:16]>C(Cl)Cl>[C:5]([N:4]([CH:1]([CH3:3])[CH3:2])[C:15]([Cl:17])=[O:16])([CH3:7])=[CH2:6]

Komponenten

5

Edukt 3

HCID 6371PhosgeneHCID 8471TriethylamineHCID 1378922-Propanamine, N-(1-methylethylidene)-

Produkt 1

HCID 2142189827676-61-5

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

99 parts of acetone isopropylimine and 94 parts of triethylamine are dissolved in 400 parts of methylene chloride, and the whole reacted with 120 parts of phosgene at a temperature of 30° to 40° C., as described in Example 1. After isolation, 131 parts (81% of the theory) of N-isopropenyl-N-isopropylcarbamyl chloride is obtained having a boiling point of 69° C. at 3 mm.

Quellen und Nachweise

ORD-Eintrag
ord-ce74260db5984f96846981140cc39aa4
Quelldatensatz
uspto-grants-1977_07
Patentnummer
US04038311

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