HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Nitric Acid → 2,6-Dimethyl-4-nitropyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Nitric Acid | HCID 944 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 2,6-Dimethylpyridine N-oxide | HCID 14083 | — |
| Produkt | 2,6-Dimethyl-4-nitropyridine | HCID 4327895 | — |
Reaktionsschritte
The 4-nitro substituted starting material is prepared by contacting 2,6-dimethylpyridine N-oxide with nitric acid and sulfuric acid thereby forming the 2,6-dimethyl-4-nitropyridine. The N-oxide is reduced to the pyridine compound with phosphorous trichloride and then oxidized to the 4-nitropyridine 2,6-dicarboxylic acid with potassium permanganate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04038398 |
| Quelldatensatz | uspto-grants-1977_07 |
| ORD ID | ord-c1e2f84e27b74439a7f91bfc0a9321e3 |
| Quellennotiz | uspto-grants-1977_07 |