HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Methyl-2-nitropyridin-3-ol → 2-Amino-6-methylpyridin-3-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Methyl-2-nitropyridin-3-ol | HCID 84801 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 2-Amino-6-methylpyridin-3-ol | HCID 88500 | — |
Reaktionsschritte
3-Hydroxy-6-methyl-2-nitropyridine (3.5 g.) in 75 ml. of methanol was reduced over 1 g. of 5% palladium-on-carbon catalyst. The catalyst was removed by filtration and the filtrate was concentrated to dryness to give 2-amino-3-hydroxy-6-methylpyridine which was used directly in the next stop.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04038396 |
| Quelldatensatz | uspto-grants-1977_07 |
| ORD ID | ord-dd1ed04a0aff4fbd85a039e52bf1a545 |
| Quellennotiz | uspto-grants-1977_07 |