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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 25964Erstellt: 24. Oktober 2026

Bromine → 1-Bromo-3,3-dimethyl-1-phenylbutan-2-one

https://huagongshe.com/de/reaction/25964

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBromineHCID 24408—
Edukt3,3-Dimethyl-1-phenylbutan-2-oneHCID 10171281—
LösungsmittelCarbon TetrachlorideHCID 5943—
Produkt1-Bromo-3,3-dimethyl-1-phenylbutan-2-oneHCID 1345869399,5%

Reaktionsschritte

17.6 g (0.1 mol) of 1-phenyl-3,3-dimethyl-butan-2-one were dissolved in 100 ml of carbon tetrachloride, 5 ml (0.1 mole) of bromine were added dropwise thereto while stirring and under reflux, and the mixture was heated to the boil for one hour. After cooling, the distilling off the solvent, 25.4 g of 1-bromo-1-phenyl-3,3-dimethyl-butan-2-one of melting point 38°-42° C. were obtained in quantitative yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04147791
Quelldatensatzuspto-grants-1979_04
ORD IDord-f404599ab53b42d4923b6b07a99ec118
Quellennotizuspto-grants-1979_04