HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorotrimethylsilane → 2-Benzyl-2-trimethylsilyl-1,3-dithiane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorotrimethylsilane | HCID 6397 | — |
| Edukt | 2-Benzyl-1,3-dithiane | HCID 300291 | — |
| Produkt | 2-Benzyl-2-trimethylsilyl-1,3-dithiane | HCID 10469008 | 75% |
Reaktionsschritte
The title compound of this step was prepared in 75% yield, by the procedure described in JACS 89, (1967), 4347 by E. J. Corey, et al., using 2-benzyl-1,3-dithiane and trimethylsilyl chloride. The product was recrystallized from diethyl ether/pentane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05529988 |
| Quelldatensatz | uspto-grants-1996_06 |
| ORD ID | ord-157274fec4e5454391c7c93903080036 |
| Quellennotiz | uspto-grants-1996_06 |