HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Homophthalic acid → 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Homophthalic acid | HCID 66643 | — |
| Edukt | Sodium Acetate | HCID 517045 | — |
| Edukt | 2-Amino-2-methylpropane-1-thiol | HCID 521040 | — |
| Lösungsmittel | 1,2-Dichlorobenzene | HCID 7239 | — |
| Produkt | 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline | HCID 12593065 | — |
Reaktionsschritte
By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04163844 |
| Quelldatensatz | uspto-grants-1979_08 |
| ORD ID | ord-64cfce68ca0c405c91b0742af24d77f8 |
| Quellennotiz | uspto-grants-1979_08 |