HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Mercaptoethanol → 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Mercaptoethanol | HCID 1567 | — |
| Edukt | ACMC-20apjz | HCID 3690897 | — |
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 2-(6-Carboxyhexyl)-4-(2-hydroxyethylthio)cyclopent-2-en-1-one | HCID 23346654 | — |
Reaktionsschritte
In the manner of Example 281 a methanol solution of 2-(6-carboxyhexyl)-4-hydroxycyclopent-2-en-1-one [Prostaglandins, 3, 921 (1973)] and β-mercaptoethanol is treated with sodium methoxide solution, acidified, concentrated, and extracted to provide the subject compound as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04165331 |
| Quelldatensatz | uspto-grants-1979_08 |
| ORD ID | ord-30160fcc15e5467ca5ce4ce942634e16 |
| Quellennotiz | uspto-grants-1979_08 |