HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Chloro-2-methylaniline → N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Chloro-2-methylaniline | HCID 6894 | — |
| Edukt | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Produkt | N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline | HCID 13017553 | — |
Reaktionsschritte
2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) are ground in a mortar. The mixture is heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gives N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline; Bp. 139° C./0/020 mm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04152452 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-1440b92d0377440f9c15e6bd3a2a2ab7 |
| Quellennotiz | uspto-grants-1979_05 |