HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichloroaniline → Triclocarban
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichloroaniline | HCID 7257 | — |
| Edukt | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Edukt | Isocyanate | HCID 105034 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Triclocarban | HCID 7547 | — |
Reaktionsschritte
A cold solution of 3,4-dichloroaniline (13.2 parts) in chloroform 75 parts was added to the isocyanate solution from A (120 parts containing 7.5 parts of 4-chlorophenyl isocyanate). The mixture was stirred at room temperature for 16 hours, then the solid filtered off, washed with chloroform and dried.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04153624 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-7ae4cd751f7140aa9f83d2532c6685d9 |
| Quellennotiz | uspto-grants-1979_05 |