HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Phenylhydroxylamine → 1-(4-chlorophenyl)-N-phenylmethanimine oxide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Phenylhydroxylamine | HCID 7518 | — |
| Edukt | N-(p-Chlorobenzylidene)-2-methyl-4-chloroaniline | HCID 13017552 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 1-(4-chlorophenyl)-N-phenylmethanimine oxide | HCID 254504 | — |
Reaktionsschritte
N-phenylhydroxylamine (0.052 mole) was dissolved in ether (20 cc). This solution was treated with N-(p-chlorobenzylidene)-2-methyl-4-chloroaniline (13.8 g.) dissolved in ether (50 cc). After 15 min., white crystals had begun to form. Filtration and washing with ether gave α-p-chlorophenyl-N-phenylnitrone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04153722 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-f81de597eb9f42ee8e5e409731ec805e |
| Quellennotiz | uspto-grants-1979_05 |