HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Amino-1-phenylpyrazole → 1-phenyl-1H-pyrazol-3-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Amino-1-phenylpyrazole | HCID 98736 | — |
| Katalysator | Cuprous chloride | HCID 62652 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 1-phenyl-1H-pyrazol-3-amine | HCID 594320 | 79% |
Reaktionsschritte
Example 1 was repeated using the following amounts of reagents: 5 g (0.031 mole) of 1-phenyl-3-amino-2-pyrazoline were suspended in 25 ml of ethanol and 2 ml of H2O, under addition of 0.1 g (0.001 mole) of CuCl and 0.064 g (0.001 mole) of Cu, under an oxygen head. Oxidation lasted about 3 hours. 3.9 g of 1-phenyl-3-aminopyrazole were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04149005 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-c92401cf0af74139875db1b812c748f5 |
| Quellennotiz | uspto-grants-1979_04 |