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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 26272Erstellt: 25. Oktober 2026

3-Amino-1-phenylpyrazole → 1-phenyl-1H-pyrazol-3-amine

https://huagongshe.com/reaction/26272

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Amino-1-phenylpyrazoleHCID 98736—
KatalysatorCuprous chlorideHCID 62652—
LösungsmittelEthanolHCID 702—
LösungsmittelWaterHCID 962—
Produkt1-phenyl-1H-pyrazol-3-amineHCID 59432079%

Reaktionsschritte

Example 1 was repeated using the following amounts of reagents: 5 g (0.031 mole) of 1-phenyl-3-amino-2-pyrazoline were suspended in 25 ml of ethanol and 2 ml of H2O, under addition of 0.1 g (0.001 mole) of CuCl and 0.064 g (0.001 mole) of Cu, under an oxygen head. Oxidation lasted about 3 hours. 3.9 g of 1-phenyl-3-aminopyrazole were obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04149005
Quelldatensatzuspto-grants-1979_04
ORD IDord-c92401cf0af74139875db1b812c748f5
Quellennotizuspto-grants-1979_04