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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2632Erstellt: 23. Oktober 2026

1,2-Benzenedicarbonitrile, 4-nitro- → 4-Phenoxyphthalonitrile

https://huagongshe.com/de/reaction/2632

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-Benzenedicarbonitrile, 4-nitro-HCID 97443—
EduktPhenolate SodiumHCID 4445035—
LösungsmittelDimethylformamideHCID 6228—
Produkt4-PhenoxyphthalonitrileHCID 37180049%

Reaktionsschritte

The procedure of Example 35 was followed except that 1,2-dicyano-4-nitrobenzene (1.0 part) was used in place of the 1,2-dicyano-3-nitrobenzene, 1.0 parts instead of 2.79 parts of sodium phenoxide and 20 parts instead of 50 parts of dimethylformamide were used. 1,2-Dicyano-4-phenoxybenzene (0.6 parts, 49%) was obtained as a white solid, m.pt.98°-100° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05730759
Quelldatensatzuspto-grants-1998_03
ORD IDord-690d3f8480e44e9f98c5d08baf524723
Quellennotizuspto-grants-1998_03