HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl Gentisate → Methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl Gentisate | HCID 75077 | — |
| Edukt | 3,5,5-Trimethylhexyl p-toluenesulfonate | HCID 19036683 | — |
| Produkt | Methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate | HCID 19036700 | 76% |
Reaktionsschritte
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 3,5,5-trimethylhexyl p-toluenesulfonate, to obtain methyl 5-(3,5,5-trimethylhexyloxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 10) as a colorless, clear and oily substance in a yield of 76%. The analytical results are shown below. ##STR31##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05646184 |
| Quelldatensatz | uspto-grants-1997_07 |
| ORD ID | ord-2fd0cb85959e4ba889eb5e6891fecc2f |
| Quellennotiz | uspto-grants-1997_07 |