Hydrochloric Acid → Diethyl 2-acetoxymethylimidazole-4,5-dicarboxylate
Reaktionsgleichung
[C:1]([O:4][CH2:5][C:6]1[N:7](CC2C=CC=CC=2)[C:8]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:9]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[N:10]=1)(=[O:3])[CH3:2].Cl>>[C:1]([O:4][CH2:5][C:6]1[NH:10][C:9]([C:11]([O:13][CH2:14][CH3:15])=[O:12])=[C:8]([C:16]([O:18][CH2:19][CH3:20])=[O:17])[N:7]=1)(=[O:3])[CH3:2]Komponenten
3
Versuchsvorschrift
Following a procedure similar to that described in Preparation 42(iv), but using 2.00 g of diethyl 2-acetoxymethyl-1-benzylimidazole-4,5-dicarboxylate [prepared as described in step (i) above] as a starting material, 1.70 g of the hydrochloride of the title compound were obtained as a syrup.
Aufarbeitung
- customprepared
Quellen und Nachweise
- ORD-Eintrag
- ord-35d2f2878c8c4035b41f3e55aa559f6d