HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → Methyl 7-(3,4,5-triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)-5-heptynoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| Edukt | Methyl 7-bromohept-5-ynoate | HCID 11287432 | — |
| Lösungsmittel | Methyl Ethyl Ketone | HCID 6569 | — |
| Produkt | Methyl 7-(3,4,5-triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)-5-heptynoate | HCID 22916387 | — |
Reaktionsschritte
1,4,5-Triphenylimidazol-2-one was treated with methyl 7-bromo-5-heptynoate and potassium carbonate in butanone to give after work-up the title compound, m.p. 133°-134° C.,
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05648373 |
| Quelldatensatz | uspto-grants-1997_07 |
| ORD ID | ord-0067579590f343b9a1ae3b5e185747d6 |
| Quellennotiz | uspto-grants-1997_07 |