HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | Nafimidone monohydrochloride | HCID 51199 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone | HCID 51200 | — |
Reaktionsschritte
1-(2-Naphthoylmethyl)imidazole hydrochloride (1.0 g.) suspended in 50 ml. of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-(2-naphthoylmethyl)imidazole.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04150153 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-db5c8d01e01c4b6882b725e1358bba66 |
| Quellennotiz | uspto-grants-1979_04 |