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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 266191Erstellt: 24. Oktober 2026

16-Hydroxyhexadecanoic acid → 2-Dimethylaminopyridine

https://huagongshe.com/de/reaction/266191

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt16-Hydroxyhexadecanoic acidHCID 10466—
EduktDicyclohexylcarbodiimideHCID 10868—
EduktCID 11268547HCID 11268547—
LösungsmittelTetrahydrofuranHCID 8028—
Produkt2-DimethylaminopyridineHCID 21885—

Reaktionsschritte

Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 681 mg of 16-hydroxyhexadecanoic acid, 20 ml of dry tetrahydrofuran, 516 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 661 mg of the title compound were obtained as crystals melting at 85°-86° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05650430
Quelldatensatzuspto-grants-1997_07
ORD IDord-1a28e979c7d848798395f7881fc15359
Quellennotizuspto-grants-1997_07